Course title
機器分析Ⅰ   [Instrumental AnalysisⅠ]
Course category	technology speciality courses	Requirement		Credit	2
Department		Year	2～4	Semester	3rd
Course type	3rd	Course code	022384
Instructor(s)
森 啓二, 齊藤 亜紀夫, 岡本 昭子   [MORI Keiji, SAITO Akio, OKAMOTO Akiko]
Facility affiliation	Faculty of Engineering	Office	afjgxte/L1151	Email address

Course description

This lecture will introduce the basics of (1) mass spectrometry, (2) infrared spectroscopy, (3) proton nuclear-magnetic-resonance spectroscopic method, and (4) carbon-13 nuclear-magnetic-resonance spectroscopic method. The spectroscopic analyses identifying the structure of organic compounds are indispensable means when we initiate the actual research and development. This course aims not only to understand principles of each spectroscopic method but also to have practices analyzing the series of spectra. This lecture will focus on "proton-nuclear-magnetic-resonance spectroscopic method." and develop abilities of students to rationally assign the structure of organic molecules based on the integrated information of the spectra (1)-(4).

Expected Learning

The students should understand basics of the above mentioned spectroscopic analyses and cultivate practical ability to identify the structure of organic molecules based on rational and integrated analysis of the spectroscopic methods involving (1) mass spectrometry, (2) infrared spectroscopy, (3) proton nuclear-magnetic-resonance spectroscopic method, and (4) carbon-13 nuclear-magnetic-resonance spectroscopic method.

Course schedule

Session 1: Mass spectrometry (1) Session 2: Mass spectrometry (2) Session 3: Infrared spectroscopy (1) Session 4: Infrared spectroscopy (2) Session 5: Proton nuclear-magnetic-resonance spectroscopic method (1) Session 6: Proton nuclear-magnetic-resonance spectroscopic method (2) Session 7: Proton nuclear-magnetic-resonance spectroscopic method (3) Session 8: Midterm Examination Session 9: Proton nuclear-magnetic-resonance spectroscopic method (4) Session 10: Proton nuclear-magnetic-resonance spectroscopic method (5) Session 11: Proton nuclear-magnetic-resonance spectroscopic method (6) Session 12: Proton nuclear-magnetic-resonance spectroscopic method (7) Session 13: Carbon-13 nuclear magnetic resonance spectroscopic method (1) Session 14: Carbon-13 nuclear magnetic resonance spectroscopic method (2) Session 15: Final Examination

Prerequisites

Required Text(s) and Materials

1) Spectroscopic Methods in Organic Chemistry by M. Hesse, H. Meier, B. Zeeh Kagaku Dojin, ISBN: 978-4-7598-1193-3 2) Organic Chemistry (the 8 the edition) by John McMurry (1/3) Tokyo Kagaku Dojin, ISBN: 978-4-8079-0809-7 The two text books are required when you attend the first lecture.

References

1) Identification method (the 7th edition) by the spectrum of an organic compound, Tokyo Kagaku Dojin, ISBN: 4-8079-0633-X 2) Spectroscopic analysis of organic compounds Tokyo Kagaku Dojin, ISBN: 978-4-8079-0725-0 3) Spectroscopic analysis of organic compounds 1D, 2D NMR/IR/UV/MS Takenori Kusumi, Shokabo, ISBN: 978-4-7853-3509-0

Assessment/Grading

Report (20%), Midterm and Final Exam (80%).

Message from instructor(s)

Structural determination of organic molecules based on spectroscopic analysis is an essential skill for research and development. Though it may seem difficult at the beginning, rational approaches for the structural analysis would be more interesting to the students after working on exercises repeatedly, week by week. This lecture will provide the fundamentals of the spectroscopic analysis useful for the entire field of molecular science.

Course keywords

Mass spectrometry, infrared spectroscopy, a proton nuclear magnetic resonance spectroscopic method, a carbon-13 nuclear-magnetic-resonance spectroscopic method

Office hours

Office hours: New No. 1 Hall N510B room; Monday 16:00 - 17:00

Remarks 1

Remarks 2

Related URL

http://www.tuat.ac.jp/~h_oguri

Lecture Language

Japanese

Language Subject

Last update

12/27/2019 2:19:48 PM